ISSN 2594-357X
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We developed the in-situ transmission electron microscopy (TEM) observation of the reduction of silica doped wustite. The bulk wustite including 3wt% silica was prepared. The reaction of matrix with carbon was similar to using pure wustite but the Si-rich grains did not react with carbon and some precipitates appeared inside the Sirich grain and the boundary between matrix and Si-rich phase and they appeared without using carbon. They were produced at the temperature range of 673-973K and they disappeared at higher temperature. The EDS analises showed that their component were mopstly iron.
We developed the in-situ transmission electron microscopy (TEM) observation of the reduction of silica doped wustite. The bulk wustite including 3wt% silica was prepared. The reaction of matrix with carbon was similar to using pure wustite but the Si-rich grains did not react with carbon and some precipitates appeared inside the Sirich grain and the boundary between matrix and Si-rich phase and they appeared without using carbon. They were produced at the temperature range of 673-973K and they disappeared at higher temperature. The EDS analises showed that their component were mopstly iron.
Palavras-chave
Wustite; Silica; In-situ TEM; Precipitate
Wustite; Silica; In-situ TEM; Precipitate
Como citar
Ishikawa, Nobuhiro;
Takeguchi, Masaki;
Watanabe, Shuto;
Inami., Takashi.
DYNAMIC TEM OBSERVATION OF FE PRODUCTION FROM
FEO WHICH INCLUDES SI AT THE HIGH TEMPERATURE
,
p. 1306-1309.
In: 42º Seminário de Redução de Minério de Ferro e Matérias-primas / 13º Seminário Brasileiro de Minério de Ferro / 6th International Congress on the Science and Technology of Ironmaking,
Rio de Jabeiro,
2012.
ISSN: 2594-357X
, DOI 10.5151/2594-357X-22225
